Caking prevention

Gunter
(not verified)
Posted in: , on 5. Aug. 2004 - 17:55

In one of our Water Soluble NPK production plants we are facing extreme ambient conditions (temperatures upto 46°C and relative humidity levels upto 95%). Needless to say we face a lot of problems with caking of our end products (urea based as well as ammonium nitrate based). We tried several anti-caking agents, included some that work well in our European based plants, but without satisfactory results. The production is batch wise and the product is being sized using a cage mill. Blending is done in a fluidized zone blender (Forberg). The production installation is positioned inside our bulk storage warehouse and because of the its size dehumidifying is not an option. Does anyone have tips or recommendations that could solve the problem or at least bring improvements?

Best regards to all,

Gunter

Caking Problem?

Erstellt am 5. Aug. 2004 - 09:42

Greetings Gunter,

Rather than dehumidification perhaps dilution of plant air is warranted here. Can you increase the ventilation rate into the physical plant to remove plant air more rapidly? Seeing as your processing and packaging is the culprit it seems that increasing air volume into the plant will reduce the total moisture in plant,

preheating intake air will help as well. remember that cold air is heavier than warm air.

BenP
(not verified)

Re: Caking Prevention

Erstellt am 5. Aug. 2004 - 11:42

I would suggest that you need to cool the product down to a lower temperature before storage in order to reduce moisture uptake and consequently caking.

Send me an e-mail sales@merrowscientific.com and I'll put you in touch with a supplier who has an office in Belgium who can solve your problem.

Ben

Countering Caking

Erstellt am 12. Aug. 2004 - 10:56

The question could be better addressed if there was more information about the particular problems that caking is causing. In general, the two main issues raised by caking are sticking to contact surfaces and the forming solid masses. Assuming that the use of anti-caking agents is not effective or satisfactory, the surface adhesion problem can be reduced by: - trace heating to stop condensation, fitting a liner of UHMDP as insulation and for its non-crystall bonding characteristics, or by avoiding extended duration surface contact by inducing regular surface slip, e.g storing in mass flow hoppers and affecting regular small extractions or re-cycling.

Solidification of the bulk has either to be avoided, in the case of silos and storage containers, or accepted and accomodated, as with breaking devices for big bags. To prevent the formation of strong particle bonds in a mass it is necessary to induce regular bulk deformation. This can be done by re-cycling the product, even at relatively small rates if all of the material is regularly sheared. This will not happen within the body of a mass flow hopper and is hopeless in a non-mass flow hopper if the product experiences an extended storage life. However, specially profiled hoppers can be made that does cause a degree of bulk shear to occur with relatively small amounts of flow but a more cost effective method, particularly with existing facilities, is to emloy flow inserts. This is not, however, a techique to be adopted by the amature or faint hearted, but demands considerable expertise and committment.

If the problem is commercially serious it would appear to warrent a technical review by a specialist. Free advice can only go so far.

Dr M Bradley
(not verified)

Mitigating Caking

Erstellt am 13. Aug. 2004 - 10:33

All of the above approaches have their merit, but more information on where exactly is the caking problem would help.

Is it in storage after packing, or prior to packing? If it is after packing, then I would tackle it by putting in a conditioning bin just prior to packing. This will change the interstitial air and take away some of the excess moisture to make the material more caking resistant. If it is prior to packing then maybe introducing some conditioning air on the storage bins could be enough. This would be a very cheap thing to do.

At greenwich we have a lot of expertise in caking prevention and you might find some of our latest research on the subject interesting. We publish a handbook on tackling caking problems as well as other quality issues, and we rn a short course on the subject too. if either of these might be interesting drop me an email at bm08@gre.ac.uk

Mike.

Gunter
(not verified)

Thanks

Erstellt am 13. Aug. 2004 - 02:13

I would like to express my gratitude to all of you that have taken some time to reply to my post. I really value all your input. Thanks a lot.